신청기관 ( 인 ) APPLICANT : 케이씨씨 : KCC Corporation 주소 ( 한글 ) : 전라북도완주군봉동읍과학로 764 ADDRESS (ENGL.) : 764, Gwahak-ro, Bongdong-eup, Wanju-gun, Jeollabuk-do, Korea 발행면수 (PAGE) : 1 of 9 시료명세 (SAMPLE DESCRIPTION) : 시료에대한상세한정보는아래와같음 (The following submitted sample(s) said to be) 제품명 / 형식 (NAME/TYPE OF PRODUCT) 시료고유번호 (SAMPLE ID NO.) : KTMC-4300(+) : RT17R-U2146-001 (RT17R-U2146-001) 제품생산자 / 공급자 (MANUFACTURER/VENDOR) : (KCC 케이씨씨 Corporation) 시료접수일자 (SAMPLE RECEIVED) 시험일자 (TESTING DATE) 시험방법 (TEST METHOD) 시험결과 (TEST RESULT) : 2017. 12. 18. (Dec. 18, 2017) : 2017. 12. 18. ~ 2018. 01. 03. (Dec. 18, 2017~ Jan. 03, 2018) : 이시험성적서의다음페이지첨부 (Please see the following page) : 이시험성적서의다음페이지첨부 (Please see the following page) 비고 (Notes) : 1. 이시험성적서는제시된시료및시료명으로시험한결과로서유사대상시료에적용할수없음. (The test results presented in this report relate only to the object tested.) 2. 이시험성적서는승인없이복사사용을금함. (This report shall not be reproduced except in full without the written approval of the testing laboratory.) 승인자 (Approved by) 권한자 (Authorized by) Authenticity check 장준용 / 기술책임자 (Jade Jang / Lab. Technical Manager) 박병옥 / 소장 (Bo Park / Lab. General Manager)
발행면수 (PAGE) : 2 of 9 시험항목 (TEST ITEM) 브롬 (Bromine, Br) 염소 (Chlorine, Cl) 플루오르 (Fluorine, F) 요오드 (Iodine, I) 안티몬 (Antimony, Sb) 헥사브로모시클로도데칸 (Hexabromocyclododecane, HBCDD) 퍼플루오로옥타노익에시드 (Perfluorooctanoic acid, PFOA) 퍼플루오로옥탄설포네이트 (Perfluorooctane sulfonate, PFOS) 단위 (UNIT) Tested by : Hyojoo kim, Jean Kim, Sujung Lee, Yongsung Kim 분석방법 (TEST METHOD) With reference to IEC 62321-3-2 Edition 1.0 : 2013, determined by combustion IC (CIC) With reference to EN 14582, by oxygen combustion with bomb and determined by IC With reference to EN 14582, by oxygen combustion with bomb and determined by IC With reference to EN 14582, by oxygen combustion with bomb and determined by IC With reference to US EPA 3052, by acid digestion and determined by ICP-OES With reference to IEC 62321-9(111/409/CD), by solvent extraction and determined by LC/MS and GC/MS With reference to US EPA 3550C/8321B, by ultrasonic extraction and determined by LC/MS or LC/MS/MS With reference to US EPA 3550C/8321B, by ultrasonic extraction and determined by LC/MS or LC/MS/MS 검출한계 (MDL) 시험결과 (RESULT) 30 N.D. 30 190 30 N.D. 30 N.D. 2 N.D. 10 N.D. 0.1 N.D. 0.1 N.D. Notes : = ppm = parts per million ( 함량표시 : 백만분의일 ) < = Less than ( 결과값이하 ) N.D. = Not detected (< MDL, 미검출 검출한계이하 ) MDL = Method detection limit ( 검출한계 )
발행면수 (PAGE) : 3 of 9 시험항목 (TEST ITEM) 프탈레이트 (Phthalates) 디부틸프탈레이트 (Dibutyl phthalate, DBP) CAS 번호 (CAS NO.) 단위 (UNIT) 84-74-2 분석방법 (TEST METHOD) 검출한계 (MDL) 시험결과 (RESULT) 50 N.D. 디에틸헥실프탈레이트 (Di-(2-ethylhexyl) phthalate, DEHP) 디엔옥틸프탈레이트 (Di-n-octyl phthalate, DNOP) 디이소노닐프탈레이트 (Diisononyl phthalate, DINP) 디이소데실프탈레이트 (Diisodecyl phthalate, DIDP) 벤질부틸프탈레이트 (Benzyl butyl phthalate, BBP) 디이소부틸프탈레이트 (Diisobutyl phthalate, DIBP) Tested by : Sujung Lee 117-81-7 50 N.D. 117-84-0 With reference to IEC 62321-8 50 N.D. 28553-12-0 Edition 1.0 : 2017, 68515-48-0 by solvent extraction and determined by 26761-40-0 GC/MS 68515-49-1 100 100 N.D. N.D. 85-68-7 50 N.D. 84-69-5 50 N.D. Notes : = ppm = parts per million ( 함량표시 : 백만분의일 ) < = Less than ( 결과값이하 ) N.D. = Not detected (< MDL, 미검출 검출한계이하 ) MDL = Method detection limit ( 검출한계 )
발행면수 (PAGE) : 4 of 9 * 시료접수시시료상태 : (View of sample as received)
발행면수 (PAGE) : 5 of 9 Flow Chart (EN14582) Sample weighing Bomb preparation Oxygen bomb combustion Absorption solvent preparation of absorption solution Cooling, for 1hr Collection of halides make up Vol. 100mL Analyzed by IC
발행면수 (PAGE) : 6 of 9 Flow Chart (Metal Testing) Sample measurement NO Microwave digestion with HNO 3 / HCl / HF Total digestion YES Analyzed by ICP-OES ** 비고 : 이샘플은위의흐름도에따른전처리방법에의해완전용해되었음. ( The samples were dissolved totally by pre-conditioning method according to above flow chart.)
발행면수 (PAGE) : 7 of 9 Flow Chart (HBCDD) Extraction Concentration Clean up Concentration Analyzed by LC/MS and/or GC-MS
발행면수 (PAGE) : 8 of 9 Flow Chart (PFOS, PFOA) Loading in a vial Methanol loading Ultrasonication Filtering & Cleaning Make up (Methanol) Analyzed by LC/MS or LC/MS/MS
발행면수 (PAGE) : 9 of 9 Flow Chart (Phthalates) Extraction Concentration Clean-up Concentration Analyzed by GC-MS ***** End of ***** Except where explicitly agreed in writing, all work and services performed by Intertek is subject to our standard Terms and Conditions which can be obtained at our website: http://www.intertek.com/terms/. Intertek's responsibility and liability are limited to the terms and conditions of the agreement. This report is made solely on the basis of your instructions and / or information and materials supplied by you and provide no warranty on the tested sample(s) be truly representative of the sample source. The report is not intended to be a recommendation for any particular course of action, you are responsible for acting as you see fit on the basis of the report results. Intertek is under no obligation to refer to or report upon any facts or circumstances which are outside the specific instructions received and accepts no responsibility to any parties whatsoever, following the issue of the report, for any matters arising outside the agreed scope of the works. This report does not discharge or release you from your legal obligations and duties to any other person. You are the only one authorized to permit copying or distribution of this report (and then only in its entirety). Any such third parties to whom this report may be circulated rely on the content of the report solely at their own risk. This report shall not be reproduced, except in full.