첨단기술과세계표준기술의 Agilent 인증시린지필터 GC, LC, MS 를사용하는실험실에필수아이템애질런트프리미엄필터 (Certified) 많은시료를분석하는 QC/QA 실험실에적합한애질런트이코노필터 ICP-MS, ICP-OES, AA 무기물분석전필터를위한애질런트시린지필터

첨단기술과세계표준기술의 Agilent 인증시린지필터 GC, LC, MS 를사용하는실험실에필수아이템애질런트프리미엄필터 (Certified) 많은시료를분석하는 QC/QA 실험실에적합한애질런트이코노필터 ICP-MS, ICP-OES, AA 무기물분석전필터를위한애질런트시린지필터

Agilent 프리미엄시린지필터특징 1프리미엄시린지필터는 LC 또는 LC/MS로검증한데이터가들어있습니다 LC/MS Certificate LC혹은 LC/MS의보다효과적인데이터를얻기위해서는검증된시린지필터를사용해야합니다. Certified for absence of UV-absorbing substances at typical HPLC wavelength with water, methanol and acetonitrile 2 빠른필터속도와높은회수율! 유속 1bar(mL/min) 필터속도비교 : 15mm 프리미엄시린지필터 140 120 100 80 60 40 20 1bar 조건에서필터속도를비교한데이터입니다. RC(Regenerated Cellulose) 와 Nylon, 그리고 PTFE 재질의시린지필터로비교시애질런트캡티바시린지필터가탁월한빠른속도를보였습니다. 0 Agilent RC 경쟁사 RC Agilent Nylon 0.2um 경쟁사 Nylon 0.2um Agilent PTFE 경쟁사 PTFE 3 확실한컬럼수명연장효과 Column Backpressure (Bar) 900 800 700 600 샘플 : 플라즈마추출액 ( 혈장 ) 필터하지않은샘플애질런트캡티바 0.2um 시린지사용원심분리를이용한샘플 500 400 300 200 100 0 0 100 200 300 400 500 600 700 800 900 1000 주입횟수 플라즈마추출액 ( 혈장 ) 을컬럼에주입하여주입횟수에따른압력을비교하였습니다. 필터하지않았을때, 필터를했을때, 그리고원심분리만을실행하였을때의세가지경우는필터를한샘플이컬럼의압력이확연히낮았음을알수있었습니다. 컬럼 : Eclipse Plus C18 RRHD 2.1 50mm,1.8μm (PN 959757-902/ 컬럼은검출기에연결하지않고실험 ) 이동상 : Acetonitrile: Water (35:65, v/v) 유속 : 0.4 ml/min, isocratic 주입횟수 : 10 μl per injection, 1 injection per minute Column failure : 컬럼의압력 1000bar 일경우멈춤

시린지필터선택방법 STEP 1 시료가녹아있는용매유형 Aqueous 세포조직물질단백질분석거대분자분석 작은분자응용일반적수용성물질 친수성용매유기용매와섞이는용매마일드한솔벤트 유기용매산, 염기물질 PES (Polyethersulfone) ph 3~12 에서사용가능 CA (Cellulose Acetate) ph 4~8 에서사용가능 RC (Regenerated Cellulose Acetate) ph 3~12 에서사용가능 NY (Nylon) ph 3~14 에서사용가능 PTFE (Polyetra-fluorethylene) ph 1~14 에서사용가능 STEP 2 시료량에따른필터사이즈결정 지름 4mm : 1mL 이하시료 지름 15mm : 15mL 이하시료 25~28mm : 150mL 이하시료 0.1-1 ml 15 ml 10-150 ml STEP 3 LC 컬럼의입자크기에따른시린지필터공극결정 Column 입자 2μm 미만 0.2μm 공극사용 Column 입자 2μm 이상 0.2μm 혹은 0.45μm 공극사용 응용분야 첫번째추천 두번째추천 HPLC,UHPLC, LC/MS, GC Regenerated cellulose PTFE or Nylon ICP-MS PTFE Glass fiber/ptfe (High Particle samples) CE Regenerated cellulose Nylon Undiluted Organic solvents PTFE Nylon Protein 분석, 바이오물질 PES RC 혹은 CA* Tissue Culture Media PES RC 혹은 CA* 입자가많은샘플-유기용매 Glass Fiber/PTFE *RC : Regenerated cellulose CA : Cellulose acetate 입자가많은샘플-수용성용매 Glass Fiber/Nylon 필터방법 샘플링전 1mL 정도의 Air를먼저시린지에포집후샘플링을합니다. Air 는시린지필터시뒤에서시료를밀어주는역할을합니다. 샘플을시린지로채취합니다. 이때 Air는샘플위로올라가게됩니다. 시린지필터를시린지에돌려끼웁니다. 바이알에필터링을한후남아있는시료를완전히받아내기위해한번더시린지필터에공기로밀어줍니다.

시린지필터제품번호 프리미엄시린지필터 (Certified) 애질런트프리미엄시린지필터는일반용과입자가크고많은시료용이구분되어있습니다. 입자가크고많을경우유리재질의 microfiber 로 pre-filter 후 2 차필터를할수있도록 2 겹의필터처리가되어있는 2 차시린지필터로사용하는것이좋습니다. 제품번호 프리미엄필터 Pore Size( μm ) Certi 5190-5082 PTFE 4mm 100/pk 0.2 LC 5190-5083 PTFE 4mm 100/pk 0.45 LC 5190-5084 PTFE 15mm 100/pk 0.2 LC 5190-5085 PTFE 15mm 100/pk 0.45 LC 5190-5086 PTFE 25mm 100/pk 0.2 LC 5190-5087 PTFE 25mm 100/pk 0.45 LC 5190-5088 Nylon 15mm 100/pk 0.2 LC 5190-5091 Nylon 15mm 100/pk 0.45 LC 5190-5092 Nylon 25mm 100/pk 0.2 LC 5190-5093 Nylon 25mm 100/pk 0.45 LC 5190-5096 PES 15mm 100/pk 0.2 LC/MS 5190-5095 PES 4mm 100/pk 0.45 LC 5190-5094 PES 4mm 100/pk 0.2 LC/MS 5190-5097 PES 15mm 100/pk 0.45 LC 5190-5098 PES 25mm 100/pk 0.2 LC/MS 제품번호 프리미엄필터 Pore Size( μm ) Certi 5190-5099 PES 25mm 100/pk 0.45 LC 5190-5106 RegnCell 4mm 100/pk 0.2 LC 5190-5107 RegnCell 4mm 100/pk 0.45 LC 5190-5108 RegnCell 15mm 100/pk 0.2 LC 5190-5109 RegnCell 15mm 100/pk 0.45 LC 5190-5110 RegnCell 25mm 100/pk 0.2 LC 5190-5111 RegnCell 25mm 100/pk 0.45 LC 5190-5116 Celacet 28mm 100/pk 0.2 LC 5190-5117 Celacet 28mm 100/pk 0.45 LC 5190-5120 Glassfbr 28mm 100/pk LC/MS 5190-5122 Glassfbr 28mm 100/pk LC 제품번호 프리미엄 2차필터 Pore Size( μm ) Certi 5190-5126 GF/PTFE* 15mm 100/pk 0.2 LC 5190-5127 GF/PTFE 15mm 100/pk 0.45 LC 5190-5128 GF/PTFE 25mm 100/pk 0.2 LC 5190-5129 GF/PTFE 25mm 100/pk 0.45 LC 5190-5132 GF/NYLN* 15mm 100/pk 0.2 LC 5190-5133 GF/NYLN 15mm 100/pk 0.45 LC 5190-5134 GF/NYLN 25mm 100/pk 0.2 LC 5190-5135 GF/NYLN 25mm 100/pk 0.45 LC * GF/PTFE = Glass / PTFE, GF/NYLN = Glass / NYLON 이코노시린지필터 애질런트이코노필터는실험량이많고이미알고있는시료를분석하는 QC/QA 실험실에적합한필터입니다. ( 서티가포함되지않습니다 ) 일회용시린지 제품번호액세서리 9301-6476 5mL disposable syringe 100/pk 9301-6474 10mL disposable syringe 100/pk 5062-8534 20mL disposable syringes 10/pk 5mL, 10mL, 20mL 시린지끝에는 screw가되어있어필터시, 압력에의해시린지필터가분리되는현상을막아줍니다. 제품번호 이코노필터 Pore Size( μm ) 5190-5261 PVDF 13mm 1000/pk 0.2 5190-5262 PVDF 13mm 1000/pk 0.45 5190-5263 PVDF 25mm 1000/pk 0.2 5190-5264 PVDF 25mm 1000/pk 0.45 5190-5265 PTFE 13mm 1000/pk 0.2 5190-5266 PTFE 13mm 1000/pk 0.45 5190-5267 PTFE 25mm 1000/pk 0.2 5190-5268 PTFE 25mm 1000/pk 0.45 5190-5269 Nyln 13mm 1000/pk 0.2 5190-5270 Nyln 13mm 1000/pk 0.45 5190-5271 Nyln 25mm 1000/pk 0.2 5190-5272 Nyln 25mm 1000/pk 0.45 5190-5273 PES 13mm 1000/pk 0.2 5190-5274 PES 13mm 1000/pk 0.45 5190-5275 PES 25mm 1000/pk 0.2 5190-5276 PES 25mm 1000/pk 0.45 5190-5277 PP 13mm 1000/pk 0.2 5190-5278 PP 13mm 1000/pk 0.45 5190-5279 PP 25mm 1000/pk 0.2 5190-5280 PP 25mm 1000/pk 0.45 5190-5281 RegCel 13mm 1000/pk 0.2 5190-5282 RegCel 13mm 1000/pk 0.45 5190-5283 RegCel 25mm 100/pk 0.2 5190-5284 RegCel 25mm 1000/pk 0.45 제품상담 : 크로마토그래피팀 (T:02-2140-5460)

프리미엄시린지필터 Chemical Compatibility legend Compatible Limited compatibility Not compatible - Not analyzed Filter Housing N/A Polypropylene Polyethersulfone Cellulose Acetate * Polytetrafluorethylene Regnerated Cellulouse PP PES CA PTFE RC NYLON GF MBS PP Acetone - - - Acetonitrile - - N/A - Benzene - - - Benzyl alcohol - - - n-butyl acetate N/A - - - n-butanol Carbon tetrachloride - - - - Chloroform - - - Cyclohexane - Diethylacetamide - - - Diethyl ether - - Dimethyl formamide - - - Dimethylsulfoxide - - - Dioxane - - - Ethanol, 98% - Ethyl acetate - - - Ethylene glycol Formamide N/A - Gasoline Glycerin n-heptane - n-hexane - Isopropanol - Isopropyl acetate N/A - - - Methanol, 30% N/A Methanol, 98% - Methyl acetate - - - Methylene chloride - - - Methyl ethyl ketone - - - Methyl isobutyl ketone - - - Monochlorobenzene - - Pyridine - - - Tetrahydrofuran - - - Toluene - - - Trichloroethane N/A - - - N/A Xylene - - - Acids Acetic acid, 25% - - Acetic acid, 80% N/A - - - Hydrochloric acid, 20% - - - Hydrofluoric acid, 25% - - Nitric acid, 25% - - - Phosphoric acid, 1% - - Sulfuric acid, 25% - - Trichloroacetic acid, 10% N/A - - - Bases Ammonium hydroxide, 25% - Sodium hydroxide, 1N - - Aqueous solutions Formalin, 30% Hydrogen peroxide, 30% - - - Sodium hypochlorite, 5% N/A - - - ph range ph 1-14 - - - - - ph 1-13 - - - - ph 3-14 - - ph 3-12 - ph 4-8 *CA and GF s in MBS housing for 28 mm size Nylon Glass Fiber * Housing Methyacrylate Butadiene Styrene Housing polypropylene

이코노시린지필터 Chemical Compatibility legend* Recommended use R Not recommended use NR Limited Compatibility LC No instructions *This guide is only for reference. Nylon Polyvinylidene Difluoride Polytetrafluorethylene Polyethersulfone Polypropylene Regenerated Cellulose Filter NYLON PVDF PTFE PES PP RC Acetic Glacial LC R R NR R R Acetone R LC R NR R R Acetonitrile LC R R R LC R Ammonium Hydroxide, 1N R LC R R R Ammonium Hydroxide, 3N R NR R R R Amyl Acetate LC LC R R R Amyl Alcohol R R R R R R Aniline LC R R NR LC R Benzene LC LC R LC NR R Benzyl Alcohol, 100% R R R R R R Butanone LC LC R R R Butyl Acetate LC R R LC R Butyl Alcohol R R R R R R Carbon Tetrachloride LC NR R LC LC R Chloroform LC LC R NR LC R Cyclohexanone LC R NR R R Dichlorodifluoromethane, TF R R R R LC R Dichlorodifluoromethane, TMC LC LC R NR LC R Dimethyl Formamide, DMF R NR R NR R LC Dioxane R LC R R LC Ethyl Acetate LC R R LC LC R Ethyl Ether LC R R R LC R Ethylene Dichloride LR LR R NR LR Ethylene Glycol R R R LC R R Formaldehyde Solution, 30% R R R R R LC Gasoline LC LC LC R LC R Glycerol R R R LC R R Hydrochloric Concentrated NR R NR R R R Hydrochloric, 25% LC R R R R R Isopropanol R R R R R R Isopropyl Ether R R R Kerosene R R R R Methanol, 98% LC R R R R R Methyl Acetate LC LC R NR R R Methylene Chloride NR LC R NR LC R Nitric, 25% NR LC R R R Nitric, Concentrated NR LC R R NR Phenol Aqueous, 10% NR LC R NR R R Phosphoric, 25% NR R R R R Potassium hydroxide 3N R LC R R R Propylene Glycol R R R LR R R Pyridine LC LC NR NR LC R Sodium Hydroxide, 3N R LC R R R Sodium Hydroxide, 6N R NR R R R Sulfuric, Concentrated NR LC R NR R LC Tetrahydrofuran, THF R LC R NR LC LC Toluene NR LC R NR NR R Trichloroethylene LC NR R LC LC R Water R R R R R R