Thermo Orion Model 320 PerpHecT Meter
I. 1 II. A. 2 B. Keypad 3 III. A. 4 B. 4 IV. A. 5 B. 5 C. setup 6 V. ph A. 7 B. ph 8 VI. LogR ph A. 10 B. LogR? 11 C. LogR 12 VII. mv/ ORP/ A. mv 13 B. (, ) 13 VIII. T roubleshooting
A. 14 B. 15 C. 17 IX. 18 X. 19 XI. 21 XII. 22 XIII. 23 A. LogR 23 B. ph 24 C. ph 25
I. ORION ph ph ISE. ORION Model 320 ph/ mv/ ORP/ T emperature PerpHecT. P erphect A T C probe ( ) ph ORION digital LogR T M. P erphect ph, LogR ph, keypad, LED. P erphect,. ph, LogR,, ph,. 320 P erphect ph/ P erphect A g/ A g Cl (Cat N o. 9202BN ) P erphect ROS S (Cat No. 8202BN ). ORION P erph ect ROS S P erphect ph. 1
II. A. 320 LED ph.. ph, m V. set up, m an, ready LogR AT C. 2 s et up setup. L ogr LogR. setup LogR on ph. LogR. A T C AT C probe. AT C LogR. ready (ph,, m V ). AT C AT C probe, LogR LogR.. 2
B. K eypad 320 6 keypad.. m ode y es / res scroll (, ) cal setup. LogR on. ph.. ph. setup. setup. 3
III. A. P erph ect 110V (Cat. No. 020125) 220V (Cat. No. 020130).. B. 1. P erphect BNC BN C. BNC BN C (Cat. No. 090032). pin - tip. : B N C p in - tip. 2. A T C P robe AT C probe A T C. ORION AT C probe (Cat. N o. 927006 927007). 4
I V. A.. ( ) 2.,. :,. B.. P erph ect. 1. BNC shortin g cap (Cat alog No. 090045). 2. y es 3 110 V (Cat. N o. 020125). 7. 3. 0.. 4.. 5... 1. ph m ode. 7.00 0.02. 2. cal 7 ready y es. 3. SLP 100.0 y es. 100 y es. 4. ph 7.00 0.02. 5. m ode m V. 0.00 1.0. 5
C. setup set up setup setup.,. setup, y es. (, ). setup m ode. : y es. setup. S lop e. ph %. 100%.. setup., ph. y es. L ogr LogR, LogR LogR ( ON, OF F ). y es. y es. LogR ph. M anual B uff er Op tion m anual buffer option ST D 5 7 D SET 5 E 7.. y es. ST D, ph 4.01, 7.00, 10.01. SET, ph 0 ph 14. 1 ph 4. 6
V. p H A. ph.... LogR, A T C prob e. P erph ect ph. P erph ect A g/ A gcl P erphect ROS S. LogR ph. AT C. LogR A T C.. :... 7
B. p H 1. ph. 2. 4.01 7.00 7.00 10.01. 3. cal. CA L 2. y es (7-4, 7-10) y es. ph 7 ph 7.00. ready ph 7.00. y es. 4. ph 4 ( ph 10) 7.00 4.01 10.01., 4.00 10.01. ready y es. SLP 2. 5.. ready. 6. LogR AT C prob e, ph. 7.. ready, ph. : L og R, p H.. 8
: p H 7.00. 1.. 2. ph 7.00. 3. cal. CAL 2. ph 7 y es. ph 7.00. ready 7.00 y es. 4. SLP 2 100.. y es. 5.. ready. 6. LogR AT C prob e, ph. 7.. ready, ph. 9
VI. L ogr p H A. ph. ( ) ( probe ph ). ph. 1. ph., P erph ect. 2. m V ph. 25 10 3.4 %. p H 1. ph. ph 1. 1 1 p H (p H ), p H 8 ph 6 p H 9 p H 5 ph 10 p H 4 ph 11 ph 3 ph 12 ph 2 10 0.004 0.007 0.0 11 0.0 14 0.0 18 20 0.003 0.007 0.0 10 0.0 14 0.0 17 30 0.003 0.007 0.0 10 0.0 14 0.0 17 4 0 0.003 0.006 0.0 10 0.0 13 0.0 16 50 0.003 0.006 0.009 0.0 12 0.0 15 60 0.003 0.006 0.009 0.0 12 0.0 15 70 0.003 0.006 0.009 0.0 12 0.0 15 80 0.003 0.006 0.008 0.0 11 0.0 14 90 0.003 0.006 0.008 0.0 11 0.0 14 10
B. L ogr? P erphect ph ph. ORION LogR ph ph. LogR. 5. ph, ORION P erph ect. P erph ect ROS S P erph ect ph. 11
C. L ogr LogR. LogR.. 5.. 20., 20 10 30. 20, 3.,. b ath h ot plate. ph.. : L og R, L og R.,.. 1. t em p LogR LogR on y es. m ode. 2. cal LogR. CA L LogR (1- P T, 2- PT or 3- P T ). 2- PT. 3. y es y es. CA L 1. CAL 1. LogR ready. 4. CAL 1, y es. 5. CAL 2. st ep 3 4.. 6. ph. : m od e. E S C p H L og R p H. 12
VII. m V/ OR P/ A. m V 1. m ode m V. 2. BNC ORP. 3.. B. (, ) 1. AT C probe (, Cat. No. 927005, 927006). setup LogR. 2. AT C probe 3 m m phone j ack. 3. AT C prob e. LogR AT C probe... ph. 4. AT C AT C probe.. 13
VIII. T roubleshooting A. (310) y es.. (T able I ). y es. shorting cap. ( ).. : shorting cap. T e s t F un ct i on/ D i s play S e qu en c e T E ST #1 S egm ent Display.. T E ST #2 RAM Check RAM. T E ST #3 Ext ernal Input. sh ortin g cap. T E ST #4 Groun d Reference. T E ST #5 T em perature Reference referen ce. T E ST #6 Int ernal Reference referen ce. T E ST #7 Keypad T est k eypad. 0.. ready. E - 07. y es. : y es. 14
B.. 310.. E - 00 E - 07. 1 ( ). Table I E - 02 RAM Error E - 03 Error. sh ortin g cap. E - 04 Error E - 05 Reference Error E - 06 Reference Error E - 07 Keypad Error :. ( ). 15
E - 20 E - 32.. ( ). Table II E - 20 out of rang e 1.. 2.. 3.. 4.. E - 21 ABR/ ph AutoCal error ph 0.5 ph. 1. 4.01, 7.00, 10.01. 2.. 3. filling. 4.. E - 22 Calibration Std Error ph. 1.. 2.. 3.. E - 23 Bad slope ph 80 120%. 1.. 2.. 16
E - 31 Bad Value. 1.. 2... ph : 0.00 +14.00 SLP : 80% 120% T EMP : 0.0 100.0 M anual : 1 4 ph. E - 35 Bad LogR. 1. 5. - - - - E - 36 No LogR Cal LogR. 1.. 2.. - - - - - - - - - - E - 40 S erial M em ory Error. 1. 10 plug. - - - - - - - - - - C. Table III - - - - - - - - - - - - - - - - - - - - No Display lin e. - - - - - - - - - -. - - - - - - - - - - 17
IX. :,,. F CC, P art 15 S ubp ort J, Class A tes t. : OR I ON lin e F CC. CDC Cla ss A. 18
X. - - - - - - - - - - Cat alog N o. Description - - - - - - - - - - 03 1000 M odel 310 P erph ect ph/ T em perature M et er, in clu des P erph ect A g/ A gcl electrode, 115V 03 1001 M odel 310 P erph ect ph/ T em perature M et er, in clu des P erph ect A g/ A gcl electrode, 220V 0310A 0 M odel 310 P erphect ph/ T em perature M eter, in cludes P erph ect ROS S electrode, 115V 0310A 1 M odel 310 P erphect ph/ T em perature M eter, in cludes P erph ect ROS S electrode, 220V 032000 M odel 320 P erph ect ph/ m V/ T emperature M et er, inclu des P erph ect A g/ A g Cl electrode, 115V 032001 M odel 320 P erph ect ph/ m V/ T emperature M et er, inclu des P erph ect A g/ A g Cl electrode, 220V 0320A 0 M odel 320 P erphect ph/ m V/ T emperature M et er, includes P erph ect ROS S electrode, 115V 0320A 1 M odel 320 P erphect ph/ m V/ T emperature M et er, includes P erph ect ROS S electrode, 220V 033000 M odel 330 P erph ect ph/ m V/ T emperature M et er, inclu des P erph ect A g/ A g Cl electrode, 115V 033001 M odel 330 P erph ect ph/ m V/ T emperature M et er, inclu des P erph ect A g/ A g Cl electrode, 220V 0330A 0 M odel 330 P erphect ph/ m V/ T emperature M et er, includes P erph ect ROS S electrode, 115V 0330A 1 M odel 330 P erphect ph/ m V/ T emperature M et er, includes P erph ect ROS S electrode, 220V 035000 M odel 350 P erph ect ph/ m V/ Rm V/ T emperature M eter, in clu des P erph ect A g/ A gcl electrode, 115V 035001 M odel 350 P erph ect ph/ m V/ Rm V/ T emperature M eter, in clu des P erph ect A g/ A gcl electrode, 220V 0350A 0 M odel 350 P erph ect ph/ m V/ Rm V/ T emperature M et er, inclu des P erph ect ROS S electrode, 115V 0350A 1 M odel 350 P erph ect ph/ m V/ Rm V/ T emperature M et er, inclu des P erph ect ROS S electrode, 220V 0350G0 M odel 350 P erph ect ph/ m V/ Rm V/ T emperature M et er, inclu des P erph ect ROS S electrode, Print er, 115V 0350G1 M odel 350 P erph ect ph/ m V/ Rm V/ T emperature M et er, inclu des P erph ect ROS S electrode, Print er, 220V 037000 M odel 370 P erph ect ph/ ISE M eter, in cludes P erphect A g/ A gcl electrode, 115V 19
037001 M odel 370 P erph ect ph/ ISE M eter, in cludes P erphect A g/ A gcl electrode, 220V 0370A 0 M odel 370 P erph ect ph/ ISE M eter, in cludes P erphect ROS S electrode, 115V 0370A 1 M odel 370 P erph ect ph/ ISE M eter, in cludes P erphect ROS S electrode, 220V 0370G0 M odel 370 P erphect ph/ ISE M et er, in clu des P erphect ROS S electrode, Printer, 115V 0370G1 M odel 370 P erphect ph/ ISE M et er, in clu des P erphect ROS S electrode, Printer, 220V 8202BN P erph ect ROS S Glas s Com bin ation ph Electrode 8203BN P erph ect ROS S Glass S em i- m icro Com bin ation ph Electrode 8235BN P erph ect ROS S Epox y F lat Surface Com bination ph Electrode 8256BN P erph ect ROS S Epox y Com bination ph Electrode 8272BN P erph ect ROS S Glass Sure- F low Com bination ph Electrode 9202BN P erph ect ROS S Glas s Com bin ation ph Electrode 9203BN P erph ect ROS S Glass S em i- m icro Com bin ation ph Electrode 9206BN P erph ect ROS S Epox y Gel- F illed Com bination ph Electrode 9207BN P erph ect ROS S Epox y Gel- F illed T riode ph Electrode 9256BN P erph ect ROS S Epox y Com bination ph Electrode 9272BN P erph ect ROS S Glass Sure- F low Com bination ph Electrode 927005 P er ph e ct E p ox y A T C pr ob e 927006 P er ph e ct Gla s s A T C pr ob e 9 104 10 P erph ect T M buffer ph 4 in trial size 10 pack 9 107 10 P erph ect T M buffer ph 7 in trial size 10 pack 9 11010 P erph ect T M buffer ph 10 in trial size 10 pack 9 10425 P erph ect T M buffer ph 4 in trial size 10 pack 9 10725 P erph ect T M buffer ph 7 in trial size 10 pack 9 11025 P erph ect T M buffer ph 10 in trial size 10 pack - - - - - - - - - - - - - - - - 20
X I. ph 0.00 14.00 ph 0.1/ 0.01 ph 0.02 ph ( ) 80 120 % m V 1999 (L o g R ) 1000 1 1 0.1% ( ) A T C 0.0 100 0.1 1.0 L o g R (20 ) / 0.5 ph 1/ 2 9202BN P erph ect Glass Com b 8202BN 21
X II. troubleshooting,, SER IA L N O.,. ( ) 577-7 5 (135-890) TE L : (02)2140-5400( ) FA X : (02)2140-5405 TEL : 080-022 -5341 FA X : 080-022 -5342 22
X III. A. L ogr ph 3 11 LogR 0 25 20 0 25 20 p H p H 8202 0.36 0. 10 0.004 0.00 1 8203 0. 13 0.0 2 0.00 2 0.000 8235 0.04 0. 14 0.000 0.00 2 8256 0.22 0.06 0.004 0.00 1 8272 0.23 0.06 0.003 0.00 1 9202 0.2 1 0.06 0.003 0.00 1 9203 0.20 0. 10 0.00 2 0.00 1 9206 0.29 0.06 0.003 0.00 1 9207 0. 16 0.07 0.00 2 0.00 1 9256 0.27 0.07 0.003 0.00 1 9272 0.22 0.06 0.003 0.00 1 ph 3 11 LogR 0 25 20 0 25 20 p H p H 8202 0.04 0.03 0.000 0.000 8203 0.04 0.0 1 0.000 0.000 8235 0.07 0.06 0.00 1 0.00 1 8256 0.04 0.06 0.000 0.00 1 8272 0.02 0.0 1 0.000 0.000 9202 0.02 0.04 0.000 0.000 9203 0.03 0.06 0.000 0.00 1 9206 0.06 0.05 0.00 1 0.00 1 9207 0.02 0.0 2 0.000 0.000 9256 0.07 0.07 0.00 1 0.00 1 9272 0.02 0.00 0.00 1 0.000 23
ph 1. ph ( ) *? Orion ph.. 1). ( ) (Input.). 2). Input Shorting Cap (Input ). 3). (P ow er ). 4). Yes". (1). Sh ortin g Cap Input E - 3. (2). T est 7 30 E - 7. ( Yes", "No", "1st ", "2nd".) 2. ph Re s et * Reset? M et er, (default ). T rouble ( ). 520A, 525A, 720A, 920A M ode l 1. Input. 2. Input Shorting Cap. 3. (.). 4. 0. 5. Reset M eter?", "Yes". 6. Reset. 230A, 250A, 290A, 4 10A, 420A, 7 10A M ode l 1. Input. 2. Input Shorting Cap. 3. S etup. (S etup Code: 2-4) 4. S etup M ode Off S croll ( ) ON Yes. 5. M easure S etup. 6.. 24
3. ph (1). ( ). (2). Input Shorting Cap. (3). m V, m V. (m V 0.5m V.) 4). m V 0.5mV Reset. ph.,,. 12.,,. ph,. 1. ph S etting,. S en sing Ju ction. - (fillin g solution ) gel type 9107, 9206, 9207 (1) ph7 Buffer 10.( 24..) (2).. (3). T riode ph BN C DIN. - A g/ A g Cl: 9102, 9103, 9104, 9155/ 56, 9157, 9162, 9202, 9203, 9256 Ross : 8102, 8103, 8104, 8115, 8135, 8155/ 56, 8163, 8166, 8202, 8203, 8235, 8256, 8263 (1).. (2). F ill hole ( ) (A g/ A gcl - P/ N900011, Ross - P/ N810007). (3). ( ) fill hole 1cm. (4). reference junction 15 (, junction.) (5). fill hole (.). 25
(6).. (7). ph7 Buffer 10.( 24..) (8).., 9157 T riode ph BN C DIN. S u re - f lo w - ( ) Junction. A g/ A gcl - 9165, 9172, 9272 Ross - 8165, 8172, 8175, 8272 (1).. (2). F ill hole ( ) (A g/ A g Cl - P/ N900011, Ross - P/ N810007). (3). ( ) fill hole (1/ 5 ) 2 Jun ction. (4). fill hole 1cm. (5). fill hole (,.). (6).. (7). ph7 Buffer 10.( 24..) (8).. 2. ph (1)., m V. (2). Buffer, ( Ready ) m V. Buffer 7 m V 30m V, Buffer 4 7 m V 4 m V 160 180m V. - 1) 7 m V : 12m V, 4 mv : 179m V : 179m V - 12m V =167m V, 160 180m V. - 2) 7 m V : 10m V, 4 mv : 154m V : 154m V - 10m V =144m V, 160 180m V. ( ph.) 3. ph (1).. (2). S en sor. 26
(7 ) (1). (Cat. N o. 910001). (2). ph Buffer 7 200m l + KCl 1g. (7 ) - (1). F illin g hole. (2). (P/ N910001) Cap ( ). (3). Cap S ealing 4. Cle aning s olution : 0.1M H Cl HN O3 30 storage 1. M em bran e/ Junction : 0.1M H Cl 1% pepsin 15. 10% sodium hypochloride 5. : 0.1M t etrasodium EDT A 15. :. 5. Org anic S olv ent ph 1) : Org anic S olv ent 80% ph Ross Glass Body 8172BN 2) : M ethan ol Ros s Int ernal filling solution (Orion cat n o. 810007) 8:2. 2 7